Preparation and Characterization of Artisanal Jackfruit Vinegars with Different Sugar Concentrations

Authors

  • Edineide Ferreira Matos da Silva Serviço Nacional de Aprendizagem Rural da Bahia. BA, Brazil. https://orcid.org/0009-0003-9984-9812
  • Marcone Matos de Oliveira Serviço Nacional de Aprendizagem Rural da Bahia. BA, Brazil. https://orcid.org/0009-0008-9655-9808
  • Bruno Emanuel Souza Coelho Universidade Federal do Vale do São Francisco, Departamento de Engenharia Agronômica. PE, Brazil. https://orcid.org/0000-0002-4526-6369
  • Luany Caroline do Nascimento Carvalho Universidade Federal do Recôncavo da Bahia, Programa de Pós-Graduação em Ciências Agrárias. BA, Brazil. https://orcid.org/0000-0003-4007-981X
  • Ana Carolina Dias Braga Instituto Federal de Educação, Ciência e Tecnologia do Sertão Pernambucano. PE, Brazil.
  • Acácio Figueiredo Neto Universidade Federal do Vale do São Francisco, Departamento de Engenharia Agrícola. BA, Brazil. https://orcid.org/0000-0002-0326-9123

DOI:

https://doi.org/10.17921/1415-6938.2026v30n1p76-95

Abstract

The growing interest in natural, functional products obtained through sustainable processes has driven the valorization of fermented foods, including vinegar. This study highlights jackfruit (Artocarpus heterophyllus Lam.), a fruit rich in sugars and bioactive compounds, as a promising raw material for vinegar production. The objective was to develop and characterize artisanal jackfruit vinegars by evaluating different sugar concentrations (0%, 5%, 10%, 15%, and 20%) regarding fermentation efficiency and final product quality. The process included alcoholic fermentation with Saccharomyces cerevisiae and acetic fermentation with Acetobacter sp., in addition to physicochemical analyses. Parameters such as pH, titratable acidity, soluble solids, and color were evaluated. Sugar concentration significantly affected all evaluated parameters (p < 0.05). The pH decreased from 2.62 (0% and 5%) to 2.19 at 15%, with a slight increase to 2.15 at 20%. Titratable acidity increased progressively, meeting Brazilian regulatory standards. Soluble solids ranged from 3.73 to 6.27 °Brix, while alcohol content varied between 9.10% and 14.67% during fermentation. The 15% sugar concentration provided a balance between acidity (4.74 g·100 mL⁻¹), pH (2.19), and soluble solids (5.73 °Brix), indicating optimal fermentation performance. Higher sugar levels (20%) reduced fermentation efficiency due to high osmotic pressure. These results confirm the feasibility of producing artisanal jackfruit vinegar, promoting the valorization of underutilized fruits and the diversification of the fermented food industry. The optimal sugar concentration ensures a balance between process efficiency and product quality, contributing to sustainability and technological innovation in food production.

Keywords: Artocarpus heterophyllus. Biotechnology. Acetic Fermentation. Technological Innovation. Agricultural Sustainability.

Resumo

O crescente interesse por produtos naturais, funcionais e obtidos por processos sustentáveis tem impulsionado a valorização de alimentos fermentados, entre eles o vinagre. Este estudo traz destaque para a jaca (Artocarpus heterophyllus Lam.), fruta rica em açúcares e compostos bioativos, como matéria-prima promissora para produção de vinagre. O objetivo foi desenvolver e caracterizar vinagres artesanais de jaca, avaliando-se diferentes concentrações de açúcar (0%, 5%, 10%, 15% e 20%) sobre a eficiência fermentativa e a qualidade do produto final. O processo incluiu fermentação alcoólica com Saccharomyces cerevisiae e acética com Acetobacter sp., além de análises físico-químicas. Parâmetros como pH, acidez titulável, sólidos solúveis e cor foram avaliados. A concentração de açúcar afetou significativamente todos os parâmetros avaliados (p < 0,05). O pH diminuiu de 2,62 (0% e 5%) para 2,19 em 15%, com um leve aumento para 2,15 em 20%. A acidez titulável aumentou progressivamente, atendendo aos padrões regulamentares brasileiros. Os sólidos solúveis variaram de 3,73 a 6,27 °Brix, enquanto o teor alcoólico variou entre 9,10% e 14,67% durante a fermentação. A concentração de açúcar de 15% proporcionou um equilíbrio entre acidez (4,74 g·100 mL⁻¹), pH (2,19) e sólidos solúveis (5,73 °Brix), indicando desempenho ótimo da fermentação. Níveis mais altos de açúcar (20%) reduziram a eficiência fermentativa devido à alta pressão osmótica. Esses resultados confirmam a viabilidade da produção de vinagre artesanal de jaca, promovendo a valorização de frutas subutilizadas e a diversificação da indústria de alimentos fermentados. A concentração ideal garante um equilíbrio entre eficiência do processo e qualidade do produto, contribuindo para a sustentabilidade e inovação tecnológica na produção de alimentos.

Palavras-chave: Artocarpus heterophyllus. Biotecnologia. Fermentação Acética. Inovação Tecnológica. Sustentabilidade Agrícola.

Downloads

Download data is not yet available.

Author Biographies

Edineide Ferreira Matos da Silva, Serviço Nacional de Aprendizagem Rural da Bahia. BA, Brazil.

Technician in Fruit Science and Technician in Agribusiness, Serviço Nacional de Aprendizagem Rural da Bahia (SENAR/BA).

Marcone Matos de Oliveira, Serviço Nacional de Aprendizagem Rural da Bahia. BA, Brazil.

Technician in Fruit Science and Technician in Agribusiness, Serviço Nacional de Aprendizagem Rural da Bahia (SENAR/BA).

Bruno Emanuel Souza Coelho, Universidade Federal do Vale do São Francisco, Departamento de Engenharia Agronômica. PE, Brazil.

Master’s degree in Agronomy – Crop Science, with emphasis on Production, Management, and Postharvest, from the Federal University of the São Francisco Valley (Univasf) (2022). Specialist in Postharvest of Horticultural Products from the Federal Institute of the Sertão Pernambucano (IF Sertão-PE) (2024), in Quality Management and Food Technology from the Federal Institute of Paraná (IFPR) (2023), and in Food Science, in the area of Fruit and Vegetable Technology, from the Federal University of Pelotas (UFPel) (2022). Holds a Bachelor’s degree in Agronomic Engineering from the Federal University of the São Francisco Valley (Univasf) (2019) and a technical qualification in Food and Beverages from Senai Technical School of Petrolina (2011).

 

Luany Caroline do Nascimento Carvalho, Universidade Federal do Recôncavo da Bahia, Programa de Pós-Graduação em Ciências Agrárias. BA, Brazil.

Master’s student in Agricultural Sciences in the Graduate Program in Agricultural Sciences at the Federal University of Recôncavo of Bahia (UFRB). Holds a Bachelor’s degree in Bioprocess Engineering and Biotechnology from the State University of Bahia (UNEB). During undergraduate studies, participated in scientific initiation projects in the areas of Food and Beverage Technology, served as a teaching assistant in the Plant Physiology course, and was involved in extension projects and activities in a Junior Enterprise. Currently, is a member of the Insecta Research Group. Has experience in the field of Food Science, with emphasis on the production and quality of beverages and fermented foods.

Ana Carolina Dias Braga, Instituto Federal de Educação, Ciência e Tecnologia do Sertão Pernambucano. PE, Brazil.

Holds a Bachelor’s degree in Food Technology from the Federal Institute of Education, Science and Technology of the Sertão Pernambucano (2004), a specialization in Processing of Fruit and Vegetable Products from the same institution (2008), and a Master’s degree in Irrigated Horticulture (Plant Physiology and Postharvest of Horticultural Crops) from the State University of Bahia (2014). She is a Basic, Technical and Technological Education (EBTT) Professor at the Federal Institute of Education, Science and Technology of the Sertão Pernambucano, in the area of Agroindustry, currently assigned to the Petrolina Rural Zone Campus. She has experience in the areas of drying and storage of agricultural products, beverage technology, and development and processing of plant-based products.

Acácio Figueiredo Neto , Universidade Federal do Vale do São Francisco, Departamento de Engenharia Agrícola. BA, Brazil.

Holds a Bachelor’s degree in Agronomic Engineering from the Federal University of Paraíba (2000), a Master’s degree in Agricultural Engineering from the Federal University of Campina Grande (2003), and a PhD in Agricultural Engineering through a joint program between the Federal University of Viçosa (UFV) and the Federal University of Campina Grande (UFCG) (2012). He is currently an Associate Professor at the Federal University of the São Francisco Valley (Univasf). He has experience in the fields of Agronomy and Agricultural Engineering, with emphasis on Good Agricultural Practices (GAP) and logistics for the storage of agricultural products, working mainly on the following topics: quality control of fruits, vegetables, and grains; management of rural properties in the storage and drying sectors; and postharvest technology of seeds, vegetables, and tropical fruits.

References

ABID, J. et al. Acetic fermentation and health effects: an in-depth examination of grain vinegars and their production technologies: a review. CyTA – J. Food, v.22, p.2393758, 2024. doi: https://doi.org/10.1080/19476337.2024.2393758

BOASIAKO, T.A. et al. Advancing sustainable innovations in mulberry vinegar production: a critical review on non-thermal pre-processing technologies. Sustainability, v.16, p.1185, 2024. doi: https://doi.org/10.3390/su16031185

CHALCHISA, T.; DEREJE, B. From waste to food: Utilization of pineapple peels for vinegar production. MOJ Food Process. Technol., v.9, p.1-5, 2021. doi: https://doi.org/10.15406/mojfpt.2021.09.00254

DAI, Y. et al. Recent applications and prospects of enzymes in quality and safety control of fermented foods. Foods, v.13, p. 3804, 2024. doi: https://doi.org/10.3390/foods13233804

DE VUYST, L.; LEROY, F. Functional role of yeasts, lactic acid bacteria and acetic acid bacteria in cocoa fermentation processes. FEMS Microbiol. Rev., v.44, p.432-453, 2020. doi: https://doi.org/10.1093/femsre/fuaa014

FERREIRA, D. F. SISVAR: A computer analysis system to fixed effects split plot type designs. Braz. J. Biometr.s, v.37, p.529-535, 2019. doi: https://doi.org/10.28951/rbb.v37i4.450

GOMES, R.J. et al. Acetic acid bacteria in the food industry: systematics, characteristics and applications. Food Technol Biotechnol, v.56, n.2, p.139-151, 2018. doi: https://doi.org/10.17113/ftb.56.02.18.5593.

HATA, N.N.Y. et al. Role of acetic acid bacteria in food and beverages. Food Technol. Biotechnol., v.61, p.85-103 2023. doi: https://doi.org/10.1016/j.biotechadv.2022.107911

HOANG, B.Q.; NGUYEN, H.T.; DUONG, D.N.T. Developement of lactic acid fermentation of jackfruit (Artocarpus heterophyllus) seed drink and its physicochemical and sensory properties. J. Food Sci. Technol. v.61, p.1180-1187, 2024. doi: https://doi.org/10.1007/s13197-024-05950-0

HOPPERT, L.; KÖLLING, R.; EINFALT, D. Synergistic effects of inhibitors and osmotic stress during high gravity bioethanol production from steam-exploded lignocellulosic feedstocks. Biocatal. Agricul. Biotechnol., v.43, p.102414, 2022. doi: https://doi.org/10.1016/j.bcab.2022.102414

HU, Y. et al. Effects of acetic acid fermentation on the phytochemicals content, taste and aroma of pineapple vinegar. LWT, v. 210, p.116861, 2024. doi: https://doi.org/10.1016/j.lwt.2024.116861

IAL. Instituto Adolfo Lutz. Métodos físico-químicos para análise de alimentos. São Paulo: IAL, 2008.

LEONARD, W. et al. Fermentation transforms the phenolic profiles and bioactivities of plant-based foods. Biotechnol. Adv., v.49, p.107763, 2021. doi: https://doi.org/10.1016/j.biotechadv.2021.107763

LI, C. et al. Microwave–assisted hydrothermal conversion of crop straw: Enhancing the properties of liquid product and hydrochar by varying temperature and medium. Energ. Conv. Manag.t, v.290, p.117192, 2023. doi: https://doi.org/10.1016/j.enconman.2023.117192

LISZKOWSKA, W.; BERLOWSKA, J. Yeast fermentation at low temperatures: Adaptation to changing environmental conditions and formation of volatile compounds. Molecules, v.26, p.1035, 2021. doi: https://doi.org/10.3390/molecules26041035

LUZÓN-QUINTANA, L.M.; CASTRO, R.; DURÁN-GUERRERO, E. Biotechnological processes in fruit vinegar production. foods, v.10, p. 945, 2021. doi: https://doi.org/10.3390/foods10050945

LYNCH, K.M. et al. Physiology of acetic acid bacteria and their role in vinegar and fermented beverages. Comprehen. Rev. Food Sci. Food Saf., v.18, p.587-625, 2019. doi: https://doi.org/10.1111/1541-4337.12440

MANDHARE, A. et al. Jackfruit (Artocarpus heterophyllus): a comprehensive patent review. Current Nutrition & Food Sci., v.16, p.644-665, 2020. doi: http://dx.doi.org/10.2174/1573401315666190730120759

MARTÍNEZ-SÁNCHEZ, M.D.L.A.; MARTÍNEZ-HERNÁNDEZ, G.B.; LÓPEZ-GÓMEZ, A. Extending more than one week the shelf life of fresh-cut lettuce using vinegar enriched in bioactive compounds encapsulated in α-Cyclodextrins. Foods, v.13, p.3142, 2024. doi: https://doi.org/10.3390/foods13193142

MOTA, J.; VILELA, A. Aged to perfection: the scientific symphony behind port wine, vinegar, and acetic acid bacteria. Fermentation, v.10, p.200, 2024. doi: https://doi.org/10.3390/fermentation10040200

MUHIALDIN, B.J. et al. Traditional fermented foods and beverages in Iraq and their potential for large-scale commercialization. J. Ethnic Foods, v. 9, p. 18, 2022. doi: https://doi.org/10.1186/s42779-022-00133-8

OUATTARA, A. et al. Production of Vinegar mango using Acetobacter tropicalis CRSBAN-BVA1 and CRSBAN-BVK2 Isolated from Burkina Faso. Food Nutr. Sci., v.14, p.26-37, 2023. doi: https://doi.org/10.4236/fns.2023.141003

OUSAAID, D. et al. Fruits vinegar: Quality characteristics, phytochemistry, and functionality. Molecules, v.27, p. 222, 2021. doi: https://doi.org/10.3390/molecules27010222

PRAVEENA, B. et al. A review on isolation of Acetobacter and production of vinegar from pineapple and papaya waste (peels) using Acetobacter aceti. Handbook of Research on Waste Diversion and Minimization Technologies for the Industrial Sector, p.272-287, 2021. doi: https://doi.org/10.4018/978-1-7998-4921-6.ch013

RODA, A. et al. Metabolite profiling and volatiles of pineapple wine and vinegar obtained from pineapple waste. Food Chem., v.229, p.734-742, 2017. doi: https://doi.org/10.1016/j.foodchem.2017.02.111

SABIDI, S. et al. Safety assessment of fermented jackfruit (Artocarpus heterophyllus) pulp and leaves in Sprague‐Dawley rats. Food Sci. Nutr., v.8, p.4370-4378, 2020. doi: https://doi.org/10.1002/fsn3.1734

SAELEE, N.; CHEONG, L. Z.; CHAIJAN, M. Optimized Acetic Acid Production by Mixed Culture of Saccharomyces cerevisiae TISTR 5279 and Gluconobacter oxydans TBRC 4013 for Mangosteen Vinegar Fermentation Using Taguchi Design and Its Physicochemical Properties. Foods, v.12, p.3256, 2023. doi: https://doi.org/10.3390/foods12173256

SARANGI, P.K. et al. The Utilization of Jackfruit (Artocarpus heterophyllus L.) Waste towards Sustainable Energy and Biochemicals: the Attainment of Zero-Waste Technologies. Sustainability, v.15, p.12520, 2023. doi: https://doi.org/10.3390/su151612520

TRČEK, J.; MIRA, N.P.; JARBOE, L.R. Adaptation and tolerance of bacteria against acetic acid. Appl. Microbiol. Biotechnol., v.99, p.6215-6229, 2015. doi: https://doi.org/10.1007/s00253-015-6762-3

VAVŘINÍK, A. et al. The production of wine vinegar using different types of acetic acid bacteria. Slovak J. Food Sci., v.16, p.556-567, 2022. doi: https://doi.org/10.5219/1723

VILELA, A. Microbial dynamics in sour–sweet wine vinegar: impacts on chemical and sensory composition. Appl. Sci., v.13, p.7366, 2023. doi: https://doi.org/10.3390/app13137366

YANG, H. et al. Molecular biology: Fantastic toolkits to improve knowledge and application of acetic acid bacteria. Biotechnol. Adv.s, v.58, p.107911, 2022. doi: https://doi.org/10.1016/j.biotechadv.2022.107911

YUAN, X. et al. Recent advances of fermented fruits: A review on strains, fermentation strategies, and functional activities. Food Chem., v.22, p.101482, 2024. doi: https://doi.org/10.1016/j.fochx.2024.101482

ZAINI, N.S.M. et al. The Nutritional, Physico-chemical, and Antioxidant Changes during the Production of Soursop Vinegar Influenced by Yeast and Aeration. Pertanika J. Trop. Agricul. Sci., v.47, n.1, p.177-189, 2024. doi: https://doi.org/10.47836/pjtas.47.1.13

ZHANG, R. et al. Flavor experiences augmentation strategy for fermented dairy products: Perspective of multimodal perception, starter and enhancer, and processing. Food Rev Int., v.40, p.2227-2255, 2024. doi: https://doi.org/10.1080/87559129.2023.2262031

Downloads

Published

2026-03-25

How to Cite

SILVA, Edineide Ferreira Matos da; OLIVEIRA, Marcone Matos de; COELHO, Bruno Emanuel Souza; CARVALHO, Luany Caroline do Nascimento; BRAGA, Ana Carolina Dias; FIGUEIREDO NETO , Acácio. Preparation and Characterization of Artisanal Jackfruit Vinegars with Different Sugar Concentrations. Ensaios e Ciência: Ciências Biológicas, Agrárias e da Saúde, [S. l.], v. 30, n. 1, p. 76–95, 2026. DOI: 10.17921/1415-6938.2026v30n1p76-95. Disponível em: https://ensaioseciencia.pgsscogna.com.br/ensaioeciencia/article/view/15101. Acesso em: 18 jun. 2026.

Issue

Section

Articles